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New Methods for Imaging Nanoscale Materials

Orientational Imaging Analysis (OIA): An atomic force microscope (AFM) can be used to image a diblock copolymer film at high magnifications where individual spherical nanodomains (15 nm across) are distinguishable (left picture), or at a much lower magnification which presents a correspondingly larger region of the film (right). In the right image, individual spheres are too small to resolve, but “grains” – regions of spheres aligned in a particular direction– appear decorated by stripes. OIA extracts the grain orientation and boundaries from such images, over an area up to 100 square microns.

IRG 2: D.E. Angelescu, C.K. Harrison, M.L. Trawick, P.M. Chaikin, R.A. Register, and D.H. Adamson

Nanotechnology, the ability to control materials at the level of atoms and molecules, holds promise for computing, communications and manufacturing applications. Manipulating bits of material 1000x smaller than the width of a human hair, however, requires new tools that measure, probe, characterize and repair these tiny devices. Current technologies which work at the nanoscale are blind to larger length scales and vice versa. Needed are methods that show rich detail at nanoscales while also seeing the larger picture. Princeton University researchers have done just this, combining advanced microscopy and computing in a technique called Orientational Imaging Analysis to characterize.

Related publication [DMR-0213706]:
D.E. Angelescu, C.K. Harrison, M.L. Trawick, P.M. Chaikin, R.A. Register, and D.H. Adamson, “Orientation Imaging Microscopy in Two-Dimensional Crystals Via Undersampled Microscopy”, Appl. Phys. A 78, 387 (2004).